Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

Base Information

Chemical Name:Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;
CAS No.:80254-20-2
Molecular Formula:CF₃O₃S*C₃₆H₃₀ClN₂O
Molecular Weight:691.17
Hs Code.:

Synonyms:Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

Suppliers and Price of Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

There total 2 articles about Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 122-01-0
4-chloro-benzoyl chloride

: 80254-01-9
N-(2-aminoethyl)dibenzoacridinium trifluoromethanesulphonate

: 80254-20-2
Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

Guidance literature:: triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(01)88894-3

Reference yield:

: 73377-38-5
5,6,8,9-tetrahydro-7-phenyldibenzoxanthyilium triflouromethanesulphonate

: 80254-20-2
Trifluoro-methanesulfonate14-[2-(4-chloro-benzoylamino)-ethyl]-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium;

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) AcOH / 1.) Et₃N / 1.) CH₂Cl₂, 1 h, 0 deg C; 2.) CH₂Cl₂, 3 h

2: 84 percent / Et₃N / CH₂Cl₂ / 3 h / 20 °C

With acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)88894-3