Technology Process of meso-β--α,α,α-tris<(o-pyvalamido)phenyl>porphyrin
There total 8 articles about meso-β--α,α,α-tris<(o-pyvalamido)phenyl>porphyrin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonia;
In
methanol; chloroform;
for 12h;
Ambient temperature;
DOI:10.1021/ja00369a041
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 70 percent / conc. HBr, conc. H2SO4 / 10 h / Heating
2: 98 percent / thionyl chloride / 1.) room temperature, 1 h, 2.) reflux
3: 70 percent / pyridine / CH2Cl2 / 12 h
4: 100 percent / NaOH / dimethylformamide / 12 h / Ambient temperature; pH 8
5: 1.) mercuric acetate, 2.) hydrogen sulfide / 1.) ethanol, room temperature, 6 h, 2.) 3 h
With
pyridine; sodium hydroxide; thionyl chloride; sulfuric acid; hydrogen sulfide; mercury(II) diacetate; hydrogen bromide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00369a041
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / thionyl chloride / 1.) room temperature, 1 h, 2.) reflux
2: 70 percent / pyridine / CH2Cl2 / 12 h
3: 100 percent / NaOH / dimethylformamide / 12 h / Ambient temperature; pH 8
4: 1.) mercuric acetate, 2.) hydrogen sulfide / 1.) ethanol, room temperature, 6 h, 2.) 3 h
With
pyridine; sodium hydroxide; thionyl chloride; hydrogen sulfide; mercury(II) diacetate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00369a041
