(5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

Base Information

Chemical Name:(5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol
CAS No.:1358581-67-5
Molecular Formula:C₁₅H₁₃BrClFO₂
Molecular Weight:360.614
Hs Code.:

Synonyms:(5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

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Chemical Property of (5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

Chemical Property:

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Technology Process of (5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

There total 5 articles about (5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium borodeuteride

: 1358580-28-5
(5-bromo-2-chloro-phenyl)-(4-ethoxy-3-fluoro-phenyl)methanone

: 1358581-67-5
(5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

Guidance literature:: With aluminum (III) chloride; trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 367-12-4
2-fluorophenol

: 1358581-67-5
(5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 5 h / Reflux

2: aluminum (III) chloride / dichloromethane / 16 h / 0 °C

3: aluminum (III) chloride; trifluoroacetic acid / tetrahydrofuran / 2 h / 20 °C / Cooling with ice

With aluminum (III) chloride; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetone;

Reference yield:

: 451-80-9
1-ethoxy-2-fluoro-benzene

: 1358581-67-5
(5-bromo-2-chloro-phenyl)-deuterio-(4-ethoxy-3-fluoro-phenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 16 h / 0 °C

2: aluminum (III) chloride; trifluoroacetic acid / tetrahydrofuran / 2 h / 20 °C / Cooling with ice

With aluminum (III) chloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;