methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

Base Information

Chemical Name:methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate
CAS No.:1064195-70-5
Molecular Formula:C₂₅H₂₅NO₆
Molecular Weight:435.477
Hs Code.:

Synonyms:methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

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Chemical Property of methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

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Technology Process of methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

There total 6 articles about methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1064195-69-2
methyl 4-(4,9-diethoxy-1,3-dioxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

: 1064195-70-5
methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2010.12.014

Reference yield:

: 18595-14-7
methyl 4-amino-3-methylbenzoate

: 1064195-70-5
methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / Reflux

2: sodium tetrahydroborate / tetrahydrofuran; methanol

With sodium tetrahydroborate; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2010.12.014

Reference yield:

: 84-66-2
Diethyl phthalate

: 1064195-70-5
methyl 4-(4,9-diethoxy-1-hydroxy-3-oxo-1,3-dihydro-2H-benzo[f]isoindol-2-yl)-3-methylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium / ethanol / 3 h / 120 °C

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / Heating / reflux

3: sodium hydroxide; water / ethanol / 1.5 h / 60 °C

4: thionyl chloride / chloroform / Heating / reflux

5: acetic acid / Heating / reflux

6: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.83 h / 0 °C

With sodium hydroxide; sodium tetrahydroborate; thionyl chloride; water; sodium; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; ethanol; chloroform; N,N-dimethyl-formamide;