4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

Base Information

Chemical Name:4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide
CAS No.:1421921-64-3
Molecular Formula:BrH*C₂₃H₂₈N₄O₂S₂
Molecular Weight:537.545
Hs Code.:

Synonyms:4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

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Chemical Property of 4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

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Technology Process of 4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

There total 5 articles about 4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(bromoacetyl)-N-methylbenzenesulfonamide

: 1421922-06-6
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

: 1421921-64-3
4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

Guidance literature:: In isopropyl alcohol; at 80 ℃; for 3h;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421921-64-3
4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid / 0.5 h / Cooling with ice

2.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

4.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

4.2: 24 h / 20 °C

5.1: isopropyl alcohol / 3 h / 80 °C

With hydrogenchloride; oxalyl dichloride; water; nitric acid; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; chloroform; ethyl acetate; isopropyl alcohol;

Reference yield:

: 1421922-03-3
(2,5-dimethyl-4-nitrophenyl)acetonitrile

: 1421921-64-3
4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylbenzenesulfonamide hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

2.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

3.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

3.2: 24 h / 20 °C

4.1: isopropyl alcohol / 3 h / 80 °C

With hydrogenchloride; oxalyl dichloride; water; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; chloroform; ethyl acetate; isopropyl alcohol;