2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

Base Information

Chemical Name:2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide
CAS No.:1421922-06-6
Molecular Formula:C₁₄H₂₁N₃S
Molecular Weight:263.407
Hs Code.:

Synonyms:2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

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Chemical Property of 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

Chemical Property:

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Technology Process of 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

There total 4 articles about 2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28860-25-5
N-methyl-N-ethylformamide

: 1421922-05-5
2-(4-amino-2,5-dimethylphenyl)ethanethioamide

: 1421922-06-6
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

Guidance literature:: N-methyl-N-ethylformamide; With oxalyl dichloride; In chloroform; at 20 ℃; for 0.166667h;

2-(4-amino-2,5-dimethylphenyl)ethanethioamide; In chloroform; at 20 ℃; for 24h;

Reference yield:

: 1421922-04-4
2-(2,5-dimethyl-4-nitrophenyl)ethanethioamide

: 1421922-06-6
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

2.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

2.2: 24 h / 20 °C

With oxalyl dichloride; water; iron; ammonium chloride; In ethanol; chloroform;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421922-06-6
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid / 0.5 h / Cooling with ice

2.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

4.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

4.2: 24 h / 20 °C

With hydrogenchloride; oxalyl dichloride; water; nitric acid; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; chloroform; ethyl acetate;