o-nitrobenzyl succinic acid monoester

Base Information

Chemical Name:o-nitrobenzyl succinic acid monoester
CAS No.:86207-76-3
Molecular Formula:C₁₁H₁₁NO₆
Molecular Weight:253.211
Hs Code.:

Synonyms:o-nitrobenzyl succinic acid monoester

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Chemical Property of o-nitrobenzyl succinic acid monoester

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Technology Process of o-nitrobenzyl succinic acid monoester

There total 1 articles about o-nitrobenzyl succinic acid monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-30-5
succinic acid anhydride

: 612-25-9
2-Nitrobenzyl alcohol

: 86207-76-3
o-nitrobenzyl succinic acid monoester

Guidance literature:: succinic acid anhydride; 2-Nitrobenzyl alcohol; With dmap; In chloroform; for 24h; Reflux; Inert atmosphere;

With hydrogenchloride; In water; pH=5;
DOI:10.1021/bm400451v

Reference yield: 70.0%

: 86207-76-3
o-nitrobenzyl succinic acid monoester

: C₁₁H₁₀ClNO₅

Guidance literature:: With thionyl chloride; at 30 - 40 ℃; for 3h;
DOI:10.2478/s11696-012-0282-8

Reference yield: 65.0%

: 86207-76-3
o-nitrobenzyl succinic acid monoester

: 613688-05-4
diphenylphosphaneylmethanethiol borane complex

: C₂₄H₂₅BNO₅PS

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; sodium hydroxide; In dichloromethane; Inert atmosphere;
DOI:10.1002/anie.201611415