Technology Process of C25H31N7O5S
There total 9 articles about C25H31N7O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium diisopropyl amide / tetrahydrofuran / -78 °C
2: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere
3: sodium hydride / acetonitrile / 2 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; sodium hydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / methanol / 5 h / 20 °C
2: sodium hydrogencarbonate / water; acetone / 2 h / 20 °C
3: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere
4: sodium hydride / acetonitrile / 2 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
methanol; water; N,N-dimethyl-formamide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: oxalyl dichloride / 4 h / 20 °C
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 20 °C
3: potassium carbonate / methanol / 5 h / 20 °C
4: sodium hydrogencarbonate / water; acetone / 2 h / 20 °C
5: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere
6: sodium hydride / acetonitrile / 2 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone; acetonitrile;