(E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

Base Information

Chemical Name:(E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine
CAS No.:1417621-00-1
Molecular Formula:C₂₈H₄₁NO₂
Molecular Weight:423.639
Hs Code.:

Synonyms:(E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

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Chemical Property of (E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

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Technology Process of (E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

There total 5 articles about (E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1392469-41-8
2-(3-(4-methoxybenzyloxy)propyl)-5-bromo-4,6-dimethylpyridine

: 86883-77-4
trans-1-dec-1-enyl boronic acid

: 1417621-00-1
(E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

Guidance literature:: 2-(3-(4-methoxybenzyloxy)propyl)-5-bromo-4,6-dimethylpyridine; With palladium diacetate; sodium carbonate; triphenylphosphine; In toluene; for 0.5h; Inert atmosphere;

trans-1-dec-1-enyl boronic acid; In ethanol; Reflux;
DOI:10.1016/j.ejmech.2012.07.049

Reference yield:

: 89856-44-0
2-amino-5-bromo-4,6-dimethylpyridine

: 1417621-00-1
(E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide; bromine; sodium nitrite / water / 1 h / 0 - 5 °C

2.1: piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: platinum(IV) oxide; triethylamine / ethanol / 3 h

4.1: palladium diacetate; sodium carbonate; triphenylphosphine / toluene / 0.5 h / Inert atmosphere

4.2: Reflux

With piperidine; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen bromide; bromine; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; sodium nitrite; In tetrahydrofuran; ethanol; water; toluene; 2.1: |Sonogashira Cross-Coupling / 4.1: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2012.07.049

Reference yield:

: 5006-57-5
3,6-dibromo-2,4-dimethylpyridine

: 1417621-00-1
(E)6-(3-(4-methoxybenzyloxy)propyl)-3-(dec-1-enyl)-2,4-dimethylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.1: platinum(IV) oxide; triethylamine / ethanol / 3 h

3.1: palladium diacetate; sodium carbonate; triphenylphosphine / toluene / 0.5 h / Inert atmosphere

3.2: Reflux

With piperidine; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; toluene; 1.1: |Sonogashira Cross-Coupling / 3.1: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2012.07.049