3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

Base Information

Chemical Name:3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester
CAS No.:1325708-32-4
Molecular Formula:C₁₉H₂₁NO₆S
Molecular Weight:391.445
Hs Code.:

Synonyms:3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

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Chemical Property of 3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

Chemical Property:

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Technology Process of 3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

There total 5 articles about 3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1177422-05-7
5-Chloro-2-(cyclopropylsulfonyl)pyridine

: 752242-26-5
methyl 3-hydroxy-5-isopropoxybenzoate

: 1325708-32-4
3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

Guidance literature:: With caesium carbonate; In ISOPROPYLAMIDE; for 8h; Reflux;

Reference yield:

: 1177422-01-3
5-chloro-2-(3-chloropropylsulfanyl)pyridine

: 1325708-32-4
3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 - 25 °C

2: potassium tert-butylate / tert-butyl alcohol / 18 h / 20 °C

3: caesium carbonate / ISOPROPYLAMIDE / 8 h / Reflux

With potassium tert-butylate; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; ISOPROPYLAMIDE; tert-butyl alcohol;

Reference yield:

: 40771-41-3
2-mercapto-5-chloro-pyridine

: 1325708-32-4
3-(6-cyclopropanesulfonylpyridin-3-yloxy)-5-isopropoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 0 °C

1.2: 0 - 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 - 25 °C

3.1: potassium tert-butylate / tert-butyl alcohol / 18 h / 20 °C

4.1: caesium carbonate / ISOPROPYLAMIDE / 8 h / Reflux

With potassium tert-butylate; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; ISOPROPYLAMIDE; N,N-dimethyl-formamide; tert-butyl alcohol;