2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:1407489-33-1
Molecular Formula:C₂₆H₃₂B₂F₂O₄
Molecular Weight:468.156
Hs Code.:

Synonyms:2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Chemical Property of 2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of 2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 1 articles about 2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1407489-31-9
4,4'-(2,2-dibromoethene-1,1-diyl)bis(fluorobenzene)

: 73183-34-3
bis(pinacol)diborane

: 1407489-33-1
2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium phenoxide; at 105 ℃; for 18h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/anie.202008113

Reference yield: 63.0%

: 106-38-7
para-bromotoluene

: 1407489-33-1
2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 4,4'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(methylbenzene)

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In 1,4-dioxane; water; at 70 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202008113

Reference yield: 42.0%

: 1407489-33-1
2,2'-(2,2-bis(4-fluorophenyl)ethene-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 211434-29-6
2,2'-dibromo-4,4',5,5'-tetramethyl-1,1'-biphenyl

: 1407489-39-7
9-[bis(4-fluorophenyl)methylene]-2,3,6,7-tetramethyl-9H-fluorene

Guidance literature:: With potassium phosphate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 80 ℃; for 6h; Reagent/catalyst; Inert atmosphere;
DOI:10.1071/CH12060