2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester

Base Information

• Chemical Name: 2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester
• CAS No.: 90926-48-0
• Molecular Formula: C₁₀H₁₄O₃
• Molecular Weight: 182.219
• Mol file: 90926-48-0.mol

Synonyms:2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester

Chemical Property of 2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester

There total 1 articles about 2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethylcyclohex-1-enylamine (13815-46-8) + propynoic acid methyl ester (922-67-8) → 2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester (90926-48-0)

Guidance literature:

Multistep reaction; (i) Et₂O, (ii) aq. HCl;

DOI:10.1021/jo01027a011

Reference yield:

2-(Cyclohex-1-enyl)-2-hydroxymethylen-essigsaeure-methylester (90926-48-0) → 1-cyclohexenylacetic acid (18294-87-6)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/jo01027a011

upstream raw materials:

N,N-dimethylcyclohex-1-enylamine

propynoic acid methyl ester

Downstream raw materials:

1-cyclohexenylacetic acid