5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole

Base Information

• Chemical Name: 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole
• CAS No.: 1329709-97-8
• Molecular Formula: C₃₁H₂₂Br₂N₂O₂
• Molecular Weight: 614.336

Synonyms:5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole

Chemical Property of 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole

Chemical Property:

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Technology Process of 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole

There total 3 articles about 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

1-(4-bromo-2-(2-methoxybenzoyl)phenyl)ethanone (1329709-96-7) → 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole (1329709-97-8)

Guidance literature:

With ammonium hydroxide; In methanol; acetic acid; at 40 ℃; for 120h;

DOI:10.1021/ol201770g

Reference yield:

2-methoxybenzoylhydrazine (7466-54-8) → 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole (1329709-97-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 96 h / 85 °C

2: lead(IV) tetraacetate / tetrahydrofuran / 7 h / 20 °C

3: ammonium hydroxide / methanol; acetic acid / 120 h / 40 °C

With lead(IV) tetraacetate; ammonium hydroxide; In tetrahydrofuran; methanol; ethanol; acetic acid;

DOI:10.1021/ol201770g

Reference yield:

(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide (1329709-95-6) → 5-bromo-1-((5-bromo-3-(2-methoxyphenyl)-2H-isoindol-1-yl)methylene)-3-(2-methoxyphenyl)-1H-isoindole (1329709-97-8)

Guidance literature:

Multi-step reaction with 2 steps

1: lead(IV) tetraacetate / tetrahydrofuran / 7 h / 20 °C

2: ammonium hydroxide / methanol; acetic acid / 120 h / 40 °C

With lead(IV) tetraacetate; ammonium hydroxide; In tetrahydrofuran; methanol; acetic acid;

DOI:10.1021/ol201770g

upstream raw materials:

(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

1-(4-bromo-2-(2-methoxybenzoyl)phenyl)ethanone

2-methoxybenzoylhydrazine

Downstream raw materials:

difluoro[5-[5-hexylthiophen-2-yl]-1-[[5-[5-hexylthiophen-2-yl]-3-(2-methoxyphenyl)-2H-isoindole-1-yl]methylene]-3-(2-methoxyphenyl)-1H-isoindolate-N₁,N₂]boron

difluoro[5-bromo-1-[[5-bromo-3-(2-methoxyphenyl)-2H-isoindole-l-yl]methylene]-3-(2-methoxyphenyl)-1H-isoindolate-N¹,N²]boron

difluoro[5-[3-hexylthiophen-2-yl]-1-[[5-[3-hexylthiophen-2-yl]-3-(2-methoxyphenyl)-2H-isoindole-1-yl]methylene]-3-(2-methoxyphenyl)-1H-isoindolate-N₁,N₂]boron

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