(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

Base Information

Chemical Name:(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide
CAS No.:1329709-95-6
Molecular Formula:C₁₆H₁₅BrN₂O₃
Molecular Weight:363.211
Hs Code.:

Synonyms:(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

Suppliers and Price of (Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

Chemical Property:

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Technology Process of (Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

There total 1 articles about (Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 7466-54-8
2-methoxybenzoylhydrazine

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1329709-95-6
(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

Guidance literature:: In ethanol; at 85 ℃; for 96h;
DOI:10.1021/ol201770g

Reference yield: 99.0%

: 1329709-95-6
(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

: 1329709-96-7
1-(4-bromo-2-(2-methoxybenzoyl)phenyl)ethanone

Guidance literature:: With lead(IV) tetraacetate; In tetrahydrofuran; at 20 ℃; for 7h;
DOI:10.1021/ol201770g

Reference yield:

: 1329709-95-6
(Z)-N'-(1-(4-bromo-2-hydroxyphenyl)ethylidene)-2-methoxybenzohydrazide

: 1329997-40-1
difluoro[5-[5-hexylthiophen-2-yl]-1-[[5-[5-hexylthiophen-2-yl]-3-(2-methoxyphenyl)-2H-isoindole-1-yl]methylene]-3-(2-methoxyphenyl)-1H-isoindolate-N₁,N₂]boron

Guidance literature:: Multi-step reaction with 4 steps

1: lead(IV) tetraacetate / tetrahydrofuran / 7 h / 20 °C

2: ammonium hydroxide / methanol; acetic acid / 120 h / 40 °C

3: boron trifluoride diethyl etherate; triethylamine / toluene / 12 h / 100 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 31 h / 90 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron trifluoride diethyl etherate; lead(IV) tetraacetate; ammonium hydroxide; triethylamine; In tetrahydrofuran; methanol; acetic acid; toluene; 4: Stille coupling;
DOI:10.1021/ol201770g