C₁₃H₁₉N₃O

Base Information

Chemical Name:C₁₃H₁₉N₃O
CAS No.:950609-43-5
Molecular Formula:C₁₃H₁₉N₃O
Molecular Weight:233.313
Hs Code.:

C<sub>13</sub>H<sub>19</sub>N<sub>3</sub>O

Synonyms:C₁₃H₁₉N₃O

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Chemical Property of C₁₃H₁₉N₃O

Chemical Property:

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Technology Process of C₁₃H₁₉N₃O

There total 10 articles about C₁₃H₁₉N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85838-94-4
N-Boc-1,2,3,6-tetrahydropyridine

: 950609-43-5
C₁₃H₁₉N₃O

Guidance literature:: Multi-step reaction with 6 steps

1.1: 92 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 18 h / 20 °C

2.1: ethanol / 6 h / Heating

2.2: 27 percent / CHCl₃ / 6 h / 20 °C

3.1: 82 percent / pyridine*SO₃; Et₃N / dimethylsulfoxide / 3 h / 5 °C

4.1: 81 percent / NaHCO₃; HONH₂*HCl / ethanol; tetrahydrofuran / 1 h / 40 °C

5.1: TBAB; aq. NaOH / CH₂Cl₂ / 5 h / 20 °C

6.1: MeSO₃H / tetrahydrofuran / 18 h / 20 °C

With sodium hydroxide; methanesulfonic acid; hydroxylamine hydrochloride; tetrabutylammomium bromide; sulfur trioxide pyridine complex; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2007.05.093

Reference yield:

: 914989-28-9
C₂₃H₃₅N₃O₅

: 950609-43-5
C₁₃H₁₉N₃O

Guidance literature:: With methanesulfonic acid; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1016/j.bmcl.2007.05.093

Reference yield:

: 694-05-3
1,2,3,6-tetrahydropyridine

: 950609-43-5
C₁₃H₁₉N₃O

Guidance literature:: Multi-step reaction with 7 steps

1.1: CHCl₃ / 12 h / 20 °C

2.1: 92 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 18 h / 20 °C

3.1: ethanol / 6 h / Heating

3.2: 27 percent / CHCl₃ / 6 h / 20 °C

4.1: 82 percent / pyridine*SO₃; Et₃N / dimethylsulfoxide / 3 h / 5 °C

5.1: 81 percent / NaHCO₃; HONH₂*HCl / ethanol; tetrahydrofuran / 1 h / 40 °C

6.1: TBAB; aq. NaOH / CH₂Cl₂ / 5 h / 20 °C

7.1: MeSO₃H / tetrahydrofuran / 18 h / 20 °C

With sodium hydroxide; methanesulfonic acid; hydroxylamine hydrochloride; tetrabutylammomium bromide; sulfur trioxide pyridine complex; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane; chloroform; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2007.05.093