2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester

Base Information

• Chemical Name: 2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester
• CAS No.: 219946-35-7
• Molecular Formula: C₁₉H₂₃NO₈
• Molecular Weight: 393.394

Synonyms:2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester

Chemical Property of 2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester

There total 1 articles about 2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

bromoacetic acid tert-butyl ester (5292-43-3) + Malonic acid allyl ester 4-nitro-benzyl ester → 2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester (219946-35-7)

Guidance literature:

With potassium hexamethylsilazane; In toluene; 1.) r.t., 30 min, 2.) reflux, 4 h;

DOI:10.1055/s-1999-2536

Reference yield: 72.0%

2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester (219946-35-7) → 2-(4-Nitrobenzyloxycarbonyl)succinic acid 4-tert-butyl ester (211689-79-1)

Guidance literature:

With dimedone; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 1h;

DOI:10.1055/s-1999-2536

Reference yield:

2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester 4-tert-butyl ester (219946-35-7) → 2-(4-Nitrobenzyloxycarbonyl)succinic acid 1-allyl ester

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 2h; Yield given; Ambient temperature;

DOI:10.1055/s-1999-2536

upstream raw materials:

bromoacetic acid tert-butyl ester

Downstream raw materials:

2-(4-Nitrobenzyloxycarbonyl)succinic acid 4-tert-butyl ester

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