C₉H₉F₄NO₂S

Base Information

Chemical Name:C₉H₉F₄NO₂S
CAS No.:1159505-77-7
Molecular Formula:C₉H₉F₄NO₂S
Molecular Weight:271.236
Hs Code.:

C<sub>9</sub>H<sub>9</sub>F<sub>4</sub>NO<sub>2</sub>S

Synonyms:C₉H₉F₄NO₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₉F₄NO₂S

Chemical Property:

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Technology Process of C₉H₉F₄NO₂S

There total 3 articles about C₉H₉F₄NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1159505-61-9
C₈H₇F₄NO₂S

: 74-88-4
methyl iodide

: 1159505-77-7
C₉H₉F₄NO₂S

Guidance literature:: With potassium carbonate; In acetone; for 8h; Reflux;

Reference yield:

: 100-46-9
benzylamine

: 1159505-77-7
C₉H₉F₄NO₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.08 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate / palladium(II) bis(trifluoromethanesulfonate) dihydrate / 1,2-dichloro-ethane / 2 h / 120 °C

3.1: potassium carbonate / acetone / 8 h / 20 °C / Reflux

With potassium carbonate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; triethylamine; N,N-dimethyl-formamide; palladium(II) bis(trifluoromethanesulfonate) dihydrate; In dichloromethane; 1,2-dichloro-ethane; acetone;

Reference yield:

: 36457-58-6
N-benzyl-1,1,1-trifluoromethanesulfonamide

: 1159505-77-7
C₉H₉F₄NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate / palladium(II) bis(trifluoromethanesulfonate) dihydrate / 1,2-dichloro-ethane / 2 h / 120 °C

2: potassium carbonate / acetone / 8 h / 20 °C / Reflux

With potassium carbonate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; N,N-dimethyl-formamide; palladium(II) bis(trifluoromethanesulfonate) dihydrate; In 1,2-dichloro-ethane; acetone;