(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

Base Information

Chemical Name:(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate
CAS No.:1383448-91-6
Molecular Formula:C₃₀H₃₄N₂O₃
Molecular Weight:470.612
Hs Code.:

Synonyms:(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

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Chemical Property of (S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

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Technology Process of (S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

There total 5 articles about (S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: C₂₁H₂₁NO₆

: 1383448-91-6
(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

Guidance literature:: In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.tetasy.2012.04.010

Reference yield:

: 79261-58-8
(S)-3,4-dihydro-1H-isoquinoline-2,3-dicarboxylic acid 2-benzyl ester

: 1383448-91-6
(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

2: dichloromethane / 20 °C

With chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/ejoc.201200303

Reference yield:

: 74163-81-8
L-Tic-OH

: 1383448-91-6
(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / 1,4-dioxane; water / 3 h / 0 - 20 °C

2: chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

3: dichloromethane / 20 °C

With chloroformic acid ethyl ester; potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1002/ejoc.201200303