(S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

Base Information

Chemical Name:(S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide
CAS No.:909572-81-2
Molecular Formula:C₂₂H₂₈N₂O
Molecular Weight:336.477
Hs Code.:

Synonyms:(S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

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Chemical Property of (S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

Chemical Property:

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Technology Process of (S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

There total 6 articles about (S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1383448-91-6
(S)-benzyl 3-(2,6-diisopropylphenylcarbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

: 909572-81-2
(S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h; under 760.051 Torr;
DOI:10.1016/j.tetasy.2012.04.010

Reference yield:

: 79261-58-8
(S)-3,4-dihydro-1H-isoquinoline-2,3-dicarboxylic acid 2-benzyl ester

: 909572-81-2
(S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

2: dichloromethane / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1002/ejoc.201200303

Reference yield:

: C₁₈H₁₆ClNO₃

: 909572-81-2
(S)-N-(2,6-diisopropylphenyl)-1,2,3,4-tetrahydroisoquinoline-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane;
DOI:10.1002/ejoc.201200303