<1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

Base Information

Chemical Name:<1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester
CAS No.:138335-66-7
Molecular Formula:C₂₆H₂₇NO₅S
Molecular Weight:465.57
Hs Code.:

Synonyms:<1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

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Chemical Property of <1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

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Technology Process of <1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

There total 5 articles about <1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 138334-88-0
<1-(4-methoxyphenyl)-2-<2-nitro-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

: 138335-66-7
<1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In methanol; for 4.5h;
DOI:10.1021/jm00082a020

Reference yield:

: 5367-28-2
5-chloro-2-nitrotoluene

: 138335-66-7
<1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 2.) DMF, RT, overnight

2: 67 percent / NaH / dimethylformamide / Ambient temperature

3: 85 percent / SnCl₂*2H₂O, conc. HCl / methanol / 4.5 h

With hydrogenchloride; sodium hydride; tin(ll) chloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a020

Reference yield:

: 7443-25-6
dimethyl 2-(4-methoxybenzylidene)malonate

: 138335-66-7
<1-(4-methoxyphenyl)-2-<2-amino-5-(phenylthio)phenyl>ethyl>propanedioic acid, dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / NaH / dimethylformamide / Ambient temperature

2: 85 percent / SnCl₂*2H₂O, conc. HCl / methanol / 4.5 h

With hydrogenchloride; sodium hydride; tin(ll) chloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a020