phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Base Information

Chemical Name:phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate
CAS No.:1375744-67-4
Molecular Formula:C₂₆H₂₆N₂O₅
Molecular Weight:446.503
Hs Code.:

Synonyms:phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Suppliers and Price of phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

There total 3 articles about phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1375744-86-7
phenyl N-{[(2-hydroxy-2-phenylethyl)[(4-methoxyphenyl)methyl]carbamoyl]-methyl}-N-methylcarbamate

: 1375744-67-4
phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 0 ℃; Molecular sieve;
DOI:10.1021/jo3007144

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 1375744-67-4
phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium perchlorate / acetonitrile / 0 °C / Reflux

2: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

3: sodium acetate; pyridinium chlorochromate / dichloromethane / 0 °C / Molecular sieve

With sodium acetate; lithium perchlorate; sodium hydrogencarbonate; pyridinium chlorochromate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile;
DOI:10.1021/jo3007144

Reference yield:

: 81316-56-5
N-<(β-hydroxy-2-phenyl)ethyl>-(4-methoxyphenyl)methylamine

: 1375744-67-4
phenyl N-({[(4-methoxyphenyl)methyl](2-oxo-2-phenethyl)carbamoyl}methyl)-N-methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

2: sodium acetate; pyridinium chlorochromate / dichloromethane / 0 °C / Molecular sieve

With sodium acetate; sodium hydrogencarbonate; pyridinium chlorochromate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo3007144