2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

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Chemical Name:2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile
CAS No.:1382041-54-4
Molecular Formula:C₁₆H₉F₈N₇
Molecular Weight:451.282
Hs Code.:

Synonyms:2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

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Chemical Property of 2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

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Technology Process of 2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

There total 5 articles about 2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1382041-50-0
4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-2-nitro-benzonitrile

: 1382041-54-4
2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

Guidance literature:: With sodium dithionite; tetrabutylammomium bromide; water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 1382041-60-2
4-ethynyl-2-nitro-benzonitrile

: 1382041-54-4
2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium L-ascorbate / copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h / 20 °C

2: sodium hydroxide; water; sodium dithionite; tetrabutylammomium bromide / tetrahydrofuran / 2 h / 20 °C

With sodium dithionite; tetrabutylammomium bromide; water; sodium L-ascorbate; sodium hydroxide; copper(ll) sulfate pentahydrate; In tetrahydrofuran; water; tert-butyl alcohol;

Reference yield:

: 79603-03-5
4-bromo-2-nitro-benzonitrile

: 1382041-54-4
2-amino-4-[1-(2-methyl-5-pentafluoroethyl-4-trifluoromethyl-2H-pyrazol-3-yl)-1H-[1,2,3]triazol-4-yl]-benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; triphenylphosphine / palladium diacetate / Reflux; Inert atmosphere

2: sodium L-ascorbate / copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h / 20 °C

3: sodium hydroxide; water; sodium dithionite; tetrabutylammomium bromide / tetrahydrofuran / 2 h / 20 °C

With sodium dithionite; tetrabutylammomium bromide; water; sodium L-ascorbate; triethylamine; triphenylphosphine; sodium hydroxide; copper(ll) sulfate pentahydrate; palladium diacetate; In tetrahydrofuran; water; tert-butyl alcohol;