2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

Base Information

Chemical Name:2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine
CAS No.:1056016-03-5
Molecular Formula:C₂₀H₂₅BClN₅O₂
Molecular Weight:413.715
Hs Code.:

Synonyms:2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

Suppliers and Price of 2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 3 raw suppliers

Chemical Property of 2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

There total 2 articles about 2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 203436-45-7
2,6-dichloro-9-isopropyl-9H-purine

: 210907-84-9
3-aminophenylboronic acid pinacolate

: 1056016-03-5
2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

Guidance literature:: With triethylamine; In butan-1-ol; at 100 ℃; for 2h;
DOI:10.1021/jm800109e

Reference yield:

: 5451-40-1
2,6 dichloropurine

: 1056016-03-5
2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 120 h / 15 - 18 °C

2: triethylamine / butan-1-ol / 24 h / 100 °C

With potassium carbonate; triethylamine; In dimethyl sulfoxide; butan-1-ol;
DOI:10.1007/s00044-012-0334-1

Reference yield: 76.0%

: 109-04-6
2-bromo-pyridine

: 1056016-03-5
2-chloro-6-[3-(tetramethyldioxaborolanyl)phenylamino]-9-iso-propylpurine

: 1056016-04-6
2-chloro-6-[3-(2-pyridyl)phenylamino]-9-iso-propylpurine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; at 100 ℃; Inert atmosphere;
DOI:10.1021/jm800109e