Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester

Base Information

Chemical Name:Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester
CAS No.:118684-28-9
Molecular Formula:C₂₉H₂₇NO₈
Molecular Weight:517.535
Hs Code.:

Synonyms:Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester

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Chemical Property of Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester

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Technology Process of Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester

There total 3 articles about Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40547-58-8
N-(4-acetyl-3-hydroxyphenyl)acetamide

: 118684-28-9
Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 6 N HCl / ethanol / Heating

2: 1) mol sieves 3A, 2) H₂ / 2) 10percent Pd/C / 1) MeOH, rt, 3 days, 2) 50 psi

3: Et₃N / CH₂Cl₂ / 6 h / Ambient temperature

With hydrogenchloride; 3 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;

Reference yield:

: 2476-29-1
4-amino-2-hydroxy-acetophenone

: 118684-28-9
Terephthalic acid 1-{2-acetyl-5-[(4-methoxycarbonyl-benzoyl)-propyl-amino]-phenyl} ester 4-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) mol sieves 3A, 2) H₂ / 2) 10percent Pd/C / 1) MeOH, rt, 3 days, 2) 50 psi

2: Et₃N / CH₂Cl₂ / 6 h / Ambient temperature

With 3 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane;