[(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

Base Information

Chemical Name:[(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene
CAS No.:93929-65-8
Molecular Formula:C₁₉H₂₈Br₂O₄
Molecular Weight:480.237
Hs Code.:

Synonyms:[(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

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Chemical Property of [(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

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Technology Process of [(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

There total 13 articles about [(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93929-64-7
(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

: 93929-65-8
[(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

Guidance literature:: With pyridinium hydrobromide perbromide; In chloroform; at 0 ℃; for 0.666667h;
DOI:10.1016/S0040-4020(01)91304-3

Reference yield:

: (3S,5S)-6-(1-ethoxyethoxy)-5-hydroxy-3-vinylhexanenitrile

: 93929-65-8
[(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / i-Pr₂NEt / CH₂Cl₂ / Ambient temperature

2: 94 percent / 75percent AcOH / 0.5 h / 35 °C

3: 83 percent / pyridine / 8 h / 0 °C

5: 1.15 mg / LiAlH₄ / diethyl ether / 60 h / 0 °C

6: 96 percent / NaH / dimethylformamide / Ambient temperature

7: 1.43 g / pyridinum bromide perbromide / CHCl₃ / 0.67 h / 0 °C

With lithium aluminium tetrahydride; pyridinium hydrobromide perbromide; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; In pyridine; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)91304-3

Reference yield:

: 93929-63-6
[(1R,2S,4S)-4-(2-Methoxy-ethoxymethoxy)-2-vinyl-cyclopentyl]-methanol

: 93929-65-8
[(1R,2R,4R)-2-(1,2-Dibromo-ethyl)-4-(2-methoxy-ethoxymethoxy)-cyclopentylmethoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaH / dimethylformamide / Ambient temperature

2: 1.43 g / pyridinum bromide perbromide / CHCl₃ / 0.67 h / 0 °C

With pyridinium hydrobromide perbromide; sodium hydride; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)91304-3