(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

Base Information

Chemical Name:(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether
CAS No.:93929-64-7
Molecular Formula:C₁₉H₂₈O₄
Molecular Weight:320.429
Hs Code.:

Synonyms:(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

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Chemical Property of (1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

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Technology Process of (1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

There total 12 articles about (1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 100-44-7
benzyl chloride

: 93929-63-6
[(1R,2S,4S)-4-(2-Methoxy-ethoxymethoxy)-2-vinyl-cyclopentyl]-methanol

: 93929-64-7
(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4020(01)91304-3

Reference yield:

: (3S,5S)-6-(1-ethoxyethoxy)-5-hydroxy-3-vinylhexanenitrile

: 93929-64-7
(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / i-Pr₂NEt / CH₂Cl₂ / Ambient temperature

2: 94 percent / 75percent AcOH / 0.5 h / 35 °C

3: 83 percent / pyridine / 8 h / 0 °C

5: 1.15 mg / LiAlH₄ / diethyl ether / 60 h / 0 °C

6: 96 percent / NaH / dimethylformamide / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; In pyridine; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)91304-3

Reference yield:

: 93929-62-5
methyl(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentanecarboxylate

: 93929-64-7
(1R,2S,4S)-4-(2-methoxyethoxymethoxy)-2-vinyl-1-cyclopentylmethyl benzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.15 mg / LiAlH₄ / diethyl ether / 60 h / 0 °C

2: 96 percent / NaH / dimethylformamide / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)91304-3