8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

Base Information

Chemical Name:8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate
CAS No.:1181265-88-2
Molecular Formula:CH₄O₃S*C₂₀H₂₀FN
Molecular Weight:389.491
Hs Code.:

Synonyms:8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

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Chemical Property of 8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

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Technology Process of 8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

There total 3 articles about 8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 75-75-2,98527-29-8
methanesulfonic acid

: 1181265-86-0
8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]octan-3-ol

: 1181265-88-2
8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

Guidance literature:: 8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]octan-3-ol; With hydrogenchloride; In water; for 1h; Reflux;

With sodium hydroxide; In water;

methanesulfonic acid; In diethyl ether;

Reference yield:

: 28957-72-4
N-benzyltropinone

: 1181265-88-2
8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; pentane / 1 h / -40 - -35 °C

1.2: 1 h / -40 - -10 °C

2.1: hydrogenchloride / water / 1 h / Reflux

With hydrogenchloride; n-butyllithium; In diethyl ether; water; pentane;

Reference yield:

: 460-00-4
1-Bromo-4-fluorobenzene

: 1181265-88-2
8-benzyl-3-(4-fluoro-phenyl)-8-aza-bicyclo[3.2.1]oct-2-ene methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; pentane / 1 h / -40 - -35 °C

1.2: 1 h / -40 - -10 °C

2.1: hydrogenchloride / water / 1 h / Reflux

With hydrogenchloride; n-butyllithium; In diethyl ether; water; pentane;