N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

Base Information

Chemical Name:N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide
CAS No.:179749-68-9
Molecular Formula:C₁₇H₂₀ClN₅O₅S
Molecular Weight:441.895
Hs Code.:

Synonyms:N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

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Chemical Property of N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

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Technology Process of N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

There total 1 articles about N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 24530-67-4
N-{3-[bis(2-hydroxyethyl)amino]-4-methoxyphenyl}acetamide

: 76874-79-8
2-amino-4-chloro-5-formyl-1,3-thiazole

: 179749-68-9
N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

Guidance literature:: 2-amino-4-chloro-5-formyl-1,3-thiazole; With nitrosylsulfuric acid; sulfuric acid; at 0 - 5 ℃;

N-{3-[bis(2-hydroxyethyl)amino]-4-methoxyphenyl}acetamide; With sulfuric acid; In water; for 4h;

With sodium chloride; potassium hydroxide; In water;
DOI:10.1016/j.dyepig.2010.07.011

Reference yield:

: 179749-68-9
N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

: 74228-25-4
3-(dicyanomethylidene)-2,3-dihydrobenzothiophene-1,1-dioxide

: 179749-69-0
C₂₈H₂₄ClN₇O₆S₂

Guidance literature:: In ethanol; for 4h; Reflux;
DOI:10.1016/j.dyepig.2010.07.011

Reference yield:

: 179749-68-9
N-(5-(bis(2-hydroxyethyl)amino)-2-((4-chloro-5-formylthiazol-2-yl)diazenyl)-4-methoxyphenyl)acetamide

: 74228-25-4
3-(dicyanomethylidene)-2,3-dihydrobenzothiophene-1,1-dioxide

: 177159-73-8
C₃₂H₂₈ClN₇O₈S₂

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 4 h / Reflux

2: 1,4-dioxane / 4 h / Reflux

In 1,4-dioxane; ethanol;
DOI:10.1016/j.dyepig.2010.07.011