C₁₈H₁₇ClO₃

Base Information

Chemical Name:C₁₈H₁₇ClO₃
CAS No.:1268246-51-0
Molecular Formula:C₁₈H₁₇ClO₃
Molecular Weight:316.784
Hs Code.:

C<sub>18</sub>H<sub>17</sub>ClO<sub>3</sub>

Synonyms:C₁₈H₁₇ClO₃

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Chemical Property of C₁₈H₁₇ClO₃

Chemical Property:

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Technology Process of C₁₈H₁₇ClO₃

There total 21 articles about C₁₈H₁₇ClO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1268246-52-1
C₁₇H₁₅ClO₃

: 1268246-51-0
C₁₈H₁₇ClO₃

Guidance literature:: palladium diacetate; In diethyl ether; at -50 - 20 ℃; Inert atmosphere;

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1268246-54-3
C₁₆H₁₃ClO₃

: 1268246-51-0
C₁₈H₁₇ClO₃

Guidance literature:: palladium diacetate; In diethyl ether; at -50 - 20 ℃; Inert atmosphere;

Reference yield:

: 1459-93-4
dimethyl Isophthalate

: 1268246-51-0
C₁₈H₁₇ClO₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydroxide / methanol / 20 °C

2.1: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: phosphorus tribromide / diethyl ether / 2 h

4.1: 4 h / 175 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

5.2: 0 - 20 °C

6.1: triethylamine / dmap / dichloromethane / 1 h / 20 °C

7.1: diethylzinc / dichloromethane; hexane / 0.5 h / -78 °C

7.2: 0.5 h / -30 °C

7.3: 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

10.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 24 h / 20 °C

11.1: CHIRALPAK AD-H / hexane; ethanol; acetic acid / Resolution of racemate

12.1: hydrogenchloride / 1,4-dioxane / 4 h / 85 °C

13.1: palladium diacetate / diethyl ether / -50 - 20 °C / Inert atmosphere

With hydrogenchloride; borane-THF; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; diethylzinc; phosphorus tribromide; sodium hydride; potassium carbonate; triethylamine; sodium hydroxide; dmap; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; hexane; dichloromethane; acetic acid; N,N-dimethyl-formamide; mineral oil;