C₁₃H₁₆BrNOS

Base Information

Chemical Name:C₁₃H₁₆BrNOS
CAS No.:1201633-89-7
Molecular Formula:C₁₃H₁₆BrNOS
Molecular Weight:314.246
Hs Code.:

Synonyms:C₁₃H₁₆BrNOS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₆BrNOS

Chemical Property:

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Technology Process of C₁₃H₁₆BrNOS

There total 1 articles about C₁₃H₁₆BrNOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 40180-80-1
3-bromo-4-methylacetophenone

: 1201633-89-7
C₁₃H₁₆BrNOS

Guidance literature:: With sulfur; toluene-4-sulfonic acid; at 130 ℃; for 7h; Inert atmosphere;

Reference yield:

: 1201633-89-7
C₁₃H₁₆BrNOS

: 1201633-84-2
2-(3-bromo-4-methylphenyl)acetic acid

Guidance literature:: C₁₃H₁₆BrNOS; With water; sodium hydroxide; In ethanol; for 4h; Reflux;

With hydrogenchloride; In water;

Reference yield:

: 1201633-89-7
C₁₃H₁₆BrNOS

: 208989-24-6
1-bromo-2-(4-methyl-3-pentylphenyl)ethane

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide; water / ethanol / 4 h / Reflux

2.1: hydrogenchloride / 3.5 h / Reflux

3.1: dimethylsulfide; borane / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

3.2: 0.5 h / 0 °C / Reflux

4.1: potassium hydroxide; tetrabutylammomium bromide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 40 °C

6.1: hydrogen bromide / water / 6 h / 130 °C

With hydrogenchloride; dimethylsulfide; borane; tetrabutylammomium bromide; water; hydrogen bromide; hydrogen; potassium hydroxide; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water;