7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine

Base Information

• Chemical Name: 7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine
• CAS No.: 1431558-74-5
• Molecular Formula: C₃₂H₂₆N₄
• Molecular Weight: 466.585

Synonyms:7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine

Chemical Property of 7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine

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Technology Process of 7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine

There total 1 articles about 7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(1-benzyl-3-cyano-4,5-diphenyl-1H-pyrrol-2-yl)carbonohydrazonoyl dicyanide (55817-67-9) + 3-Methylbenzonitrile (620-22-4) → 7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine (1431558-74-5)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; for 7h; Reflux;

DOI:10.1007/s00706-012-0847-9

Reference yield: 88.0%

7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine (1431558-74-5) + p-toluenesulfonyl chloride (98-59-9) → N-(7-benzyl-5,6-diphenyl-2-m-tolyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)-4-methylbenzenesulfonamide (1616385-15-9)

Guidance literature:

With dmap; In neat (no solvent); at 160 ℃; for 2.5h;

DOI:10.1080/10426507.2013.858253

Reference yield: 85.0%

7-benzyl-2-(3-methylphenyl)-5,6-diphenyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine (1431558-74-5) + benzenesulfonyl chloride (98-09-9) → N-(7-benzyl-5,6-diphenyl-2-m-tolyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)benzenesulfonamide (1616385-14-8)

Guidance literature:

With dmap; In neat (no solvent); at 160 ℃; for 2h;

DOI:10.1080/10426507.2013.858253

upstream raw materials:

(1-benzyl-3-cyano-4,5-diphenyl-1H-pyrrol-2-yl)carbonohydrazonoyl dicyanide

3-Methylbenzonitrile

Downstream raw materials:

N-(7-benzyl-5,6-diphenyl-2-m-tolyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)benzenesulfonamide

N-(7-benzyl-5,6-diphenyl-2-m-tolyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)-4-methylbenzenesulfonamide

N-(7-benzyl-5,6-diphenyl-2-m-tolyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)-4-chlorobenzenesulfonamide

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