ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid

Base Information

• Chemical Name: ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid
• CAS No.: 129750-86-3
• Molecular Formula: C₂₁H₃₂N₂O₅
• Molecular Weight: 392.495

Synonyms:ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid

Chemical Property of ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid

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Technology Process of ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid

There total 1 articles about ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Ethyl 2-bromopropionate (535-11-5,41978-69-2) + 1,3-dicyclohexyl barbituric acid (35824-91-0) → ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid (129750-86-3)

Guidance literature:

With potassium carbonate; In ethanol; for 20h; Heating;

DOI:10.1016/0223-5234(90)90029-3

Reference yield: 52.0%

ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid (129750-86-3) → 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid (129750-87-4)

Guidance literature:

With sodium hydroxide; In ethanol; Ambient temperature;

DOI:10.1016/0223-5234(90)90029-3

Reference yield: 38.0%

morpholine (110-91-8,99108-56-2) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid (129750-86-3) → ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-5-morpholinomethyl-perihydropyrimidin-5-yl) acetic acid (129750-88-5)

Guidance literature:

In ethanol; Heating;

DOI:10.1016/0223-5234(90)90029-3

upstream raw materials:

Ethyl 2-bromopropionate

1,3-dicyclohexyl barbituric acid

Downstream raw materials:

ethyl ester of 2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-5-morpholinomethyl-perihydropyrimidin-5-yl) acetic acid

ethyl ester of 2-methyl-2-<1,3-dicyclohexyl-2,4,6-trioxo-5-(N-methyl-N-piperazinomethyl)-perihydropyrimidin-5-yl> acetic acid

2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-perhydropyrimidin-5-yl) acetic acid

2-methyl-2-(1,3-dicyclohexyl-2,4,6-trioxo-5-methyl-perihydropyrimidin-5-yl) acetic acid

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