(1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

Base Information

Chemical Name:(1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene
CAS No.:160167-60-2
Molecular Formula:C₁₆H₁₈N₂O₄
Molecular Weight:302.33
Hs Code.:

(1R,4S)-N-<N-(Carbobenzyloxy)-L-alanyl>-2,3-oxazabicyclo<2.2.1>hept-5-ene

Synonyms:(1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

Chemical Property:

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Technology Process of (1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

There total 3 articles about (1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 160056-97-3
(S)-Nα-(benzyloxycarbonyl)alanine hydroxamic acid

: 160167-60-2
(1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

: 160057-05-6
(1S,4R)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

Guidance literature:: With tetrabutylammonium periodite; In methanol; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00095a040

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 160167-60-2
(1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 96 percent / NH₂OH*HCl, KOH / methanol

3: tetrabutylammonium periodate / methanol / 1 h

With potassium hydroxide; thionyl chloride; hydroxylamine hydrochloride; tetrabutylammonium periodite; In methanol;
DOI:10.1021/jo00095a040

Reference yield:

: 28819-05-8
(S)-2-benzyloxycarbonylamino-propionic acid methyl ester

: 160167-60-2
(1R,4S)-N--2,3-oxazabicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NH₂OH*HCl, KOH / methanol

2: tetrabutylammonium periodate / methanol / 1 h

With potassium hydroxide; hydroxylamine hydrochloride; tetrabutylammonium periodite; In methanol;
DOI:10.1021/jo00095a040