5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

Base Information

Chemical Name:5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole
CAS No.:125705-65-9
Molecular Formula:C₂₆H₂₅N₅O₅
Molecular Weight:487.515
Hs Code.:

Synonyms:5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

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Chemical Property of 5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

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Technology Process of 5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

There total 4 articles about 5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 34840-23-8
1,3-Dicarbomethoxy-S-methylisothiourea

: 125705-56-8
4-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-1,2-phenylenediamine

: 125705-65-9
5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 5h; Heating;

Reference yield:

: 5307-14-2,183870-67-9
2-nitro-1,4-phenylenediamine

: 125705-65-9
5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / dicyclohexylcarbodiimide / dimethylformamide / 16 h / Ambient temperature

2: NH₂NH₂*H₂O / Raney nickel / methanol / 0.5 h / Heating

3: 51 percent / p-toluenesulphonic acid / methanol / 5 h / Heating

With toluene-4-sulfonic acid; hydrazine hydrate; dicyclohexyl-carbodiimide; nickel; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 125705-65-9
5(6)-(α-Benzyloxycarbonyl-L-phenylalanyl)amino-2-methoxycarbonyl-amino benzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / dicyclohexylcarbodiimide / dimethylformamide / 16 h / Ambient temperature

2: NH₂NH₂*H₂O / Raney nickel / methanol / 0.5 h / Heating

3: 51 percent / p-toluenesulphonic acid / methanol / 5 h / Heating

With toluene-4-sulfonic acid; hydrazine hydrate; dicyclohexyl-carbodiimide; nickel; In methanol; N,N-dimethyl-formamide;