Technology Process of C25H48O4SSi2
There total 7 articles about C25H48O4SSi2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium molybdate; dihydrogen peroxide;
In
water;
at 0 - 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/ol400157s
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(I) bromide dimethylsulfide complex / diethyl ether; tetrahydrofuran / 0.17 h / -50 - -20 °C / Inert atmosphere
1.2: 21 h / -20 °C / Inert atmosphere
1.3: Inert atmosphere
2.1: tris(triphenylphosphine)rhodium(l) chloride; hydrogen / benzene; ethanol / 5 h / 20 °C / Inert atmosphere
3.1: pyridine; tributylphosphine / 1 h / 20 °C / Inert atmosphere
4.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
5.1: ammonium molybdate; dihydrogen peroxide / water / 6 h / 0 - 20 °C / Inert atmosphere
With
pyridine; 2,6-dimethylpyridine; ammonium molybdate; tris(triphenylphosphine)rhodium(l) chloride; copper(I) bromide dimethylsulfide complex; tributylphosphine; hydrogen; dihydrogen peroxide;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; benzene;
DOI:10.1021/ol400157s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; tributylphosphine / 1 h / 20 °C / Inert atmosphere
2: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
3: ammonium molybdate; dihydrogen peroxide / water / 6 h / 0 - 20 °C / Inert atmosphere
With
pyridine; 2,6-dimethylpyridine; ammonium molybdate; tributylphosphine; dihydrogen peroxide;
In
dichloromethane; water;
DOI:10.1021/ol400157s