4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

Base Information

Chemical Name:4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene
CAS No.:160409-46-1
Molecular Formula:C₇₈H₉₂O₄S₈Si₄
Molecular Weight:1462.46
Hs Code.:

Synonyms:4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

Suppliers and Price of 4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

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Technology Process of 4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

There total 5 articles about 4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 160409-45-0
4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

: 160409-46-1
4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

Guidance literature:: With triethyl phosphite; In neat (no solvent); at 130 ℃; for 2h;
DOI:10.1055/s-1994-25606

Reference yield:

: 930-35-8
1,3-dithiol-2-thione

: 160409-45-0
4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

: 31366-25-3
tetrathiafulvalene

: 4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[2,2']bi[[1,3]dithiolylidene]

: 160409-46-1
4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

Guidance literature:: With triethyl phosphite; In neat (no solvent); at 130 ℃; for 5h; Title compound not separated from byproducts;
DOI:10.1055/s-1994-25606

Reference yield:

: 128258-71-9
4,5-bis[(2'-hydroxyethyl)thio]1,3-dithiole-2-thione

: 160409-46-1
4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / imidazole / dimethylformamide / 16 h / 20 °C

2: 100 percent / Hg(OAc)2 / acetic acid; CHCl₃ / 16 h / 20 °C

3: 62 percent / P(OEt)3 / neat (no solvent) / 2 h / 130 °C

With 1H-imidazole; mercury(II) diacetate; triethyl phosphite; In chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1055/s-1994-25606