Technology Process of C33H37N5O6
There total 6 articles about C33H37N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/ol302850n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 10% palladium hydroxide on charcoal; hydrogen / methanol / 1 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
With
10% palladium hydroxide on charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane;
DOI:10.1021/ol302850n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium hydroxide monohydrate / tetrahydrofuran; water / 17 h / 20 °C / Inert atmosphere
2: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
3: 10% palladium hydroxide on charcoal; hydrogen / methanol / 1 h / 20 °C
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; 10% palladium hydroxide on charcoal; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol302850n
