(3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

Base Information

Chemical Name:(3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one
CAS No.:1415380-04-9
Molecular Formula:C₁₈H₁₇N₃O₇S
Molecular Weight:419.415
Hs Code.:

Synonyms:(3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

Chemical Property:

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Technology Process of (3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

There total 4 articles about (3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₉N₃O₆S

: 1415380-04-9
(3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

Guidance literature:: With Jones reagent; In acetone; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo302368y

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1415380-04-9
(3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydrogencarbonate / acetonitrile / 16 h / Inert atmosphere; Reflux

2: acetonitrile / 20 h / 20 °C / Inert atmosphere

3: lithium hexamethyldisilazane / tetrahydrofuran / 12 h / Inert atmosphere

4: Jones reagent / acetone / 2 h / 0 °C / Inert atmosphere

With Jones reagent; potassium hydrogencarbonate; lithium hexamethyldisilazane; In tetrahydrofuran; acetone; acetonitrile;
DOI:10.1021/jo302368y

Reference yield:

: 1415379-94-0
C₂₅H₃₇N₃O₇SSi

: 1415380-04-9
(3R)-3-methyl-3-(2-nitrobenzenesulfonylamino)-1-[(R)-1-phenylcarboxymethyl]azetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 12 h / Inert atmosphere

2: Jones reagent / acetone / 2 h / 0 °C / Inert atmosphere

With Jones reagent; lithium hexamethyldisilazane; In tetrahydrofuran; acetone;
DOI:10.1021/jo302368y