2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid

Base Information

• Chemical Name: 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid
• CAS No.: 1036899-61-2
• Molecular Formula: C₃₀H₄₂O₈
• Molecular Weight: 530.659

Synonyms:2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid

Chemical Property of 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid

Chemical Property:

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Technology Process of 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid

There total 1 articles about 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.1%

1,4-dibenzyl 2,5-di[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl] benzene-1,2,4,5-tetracarboxylate (1036899-84-9) → 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid (1036899-61-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 2h; under 760.051 Torr;

DOI:10.1021/jo8005446

Reference yield: 93.0%

2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid (1036899-61-2) + trimethyl orthoformate (149-73-5) → 1,4-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl] 2,5-dimethyl benzene-1,2,4,5-tetracarboxylate (1036899-89-4)

Guidance literature:

for 5h; Heating;

DOI:10.1021/jo8005446

Reference yield: 91.6%

2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxycarbonyl]terephthalic acid (1036899-61-2) + orthoformic acid triethyl ester (122-51-0) → 1,4-diethyl 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl] benzene-1,2,4,5-tetracarboxylate (1036899-94-1)

Guidance literature:

for 5h; Heating;

DOI:10.1021/jo8005446

upstream raw materials:

1,4-dibenzyl 2,5-di[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl] benzene-1,2,4,5-tetracarboxylate

Downstream raw materials:

1,4-diethyl 2,5-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl] benzene-1,2,4,5-tetracarboxylate

C₁₀H₁₄N₂*C₃₀H₄₂O₈

C₁₀H₁₄N₂*C₃₀H₄₂O₈

1,4-bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl] 2,5-dimethyl benzene-1,2,4,5-tetracarboxylate

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