(4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate

Base Information

• Chemical Name: (4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate
• CAS No.: 1345834-30-1
• Molecular Formula: C₃₉H₄₄N₈O₁₂
• Molecular Weight: 816.825
• Mol file: 1345834-30-1.mol

Synonyms:(4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate

Chemical Property of (4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate

There total 2 articles about (4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4,5-dimethoxy-2-nitrobenzyl-N-succinimidyl carbonate (1345834-32-3) + 2C2HF3O2*C19H26N6 → (4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate (1345834-30-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere; Darkness;

DOI:10.1039/c1cc13355a

Reference yield:

6-nitroveratryl alcohol (1016-58-6) → (4,5-dimethoxy-2-nitrophenyl)methyl N-[(4-{[5-({4-[({[(4,5-dimethoxy-2-nitrophenyl)methoxy]carbonyl}amino)methanimidoyl]phenyl}amino)pentyl]amino}phenyl)carboximidoyl]carbamate (1345834-30-1)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / 8 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Darkness

With triethylamine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1039/c1cc13355a

upstream raw materials:

4,5-dimethoxy-2-nitrobenzyl-N-succinimidyl carbonate

6-nitroveratryl alcohol