(S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

Base Information

Chemical Name:(S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide
CAS No.:1380585-88-5
Molecular Formula:C₂₁H₂₇BrN₂O₂S
Molecular Weight:451.428
Hs Code.:

Synonyms:(S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

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Technology Process of (S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

There total 6 articles about (S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1380585-95-4
C₂₁H₂₅BrN₂O₂S

: 1380585-88-5
(S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 4.5h; Inert atmosphere;
DOI:10.1021/ol3012056

Reference yield: 89.0%

: (S,E)-N-benzyl-N-(2-bromophenyl)-4-((tert-butylsulfinyl)imino)butanamide

: 1380585-88-5
(S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 4.5h;
DOI:10.1039/c5cc05378a

Reference yield:

: 115363-92-3
N-(2-bromophenyl)-4-hydroxybutanamide

: 1380585-88-5
(S)-N-benzyl-N-(2-bromophenyl)-4-(1,1-dimethylethylsulfinamido)butanamide

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / N,N-dimethyl-formamide; acetonitrile / 8 h / 0 - 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 6 h / 20 °C / Inert atmosphere

3: potassium hydrogensulfate / toluene / 3 h / 45 °C / Inert atmosphere

4: sodium tetrahydroborate / methanol / 4.5 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; potassium hydrogensulfate; caesium carbonate; Dess-Martin periodane; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ol3012056