tricyclohexylplumbyl-tricyclohexylstannane

Base Information

Chemical Name:tricyclohexylplumbyl-tricyclohexylstannane
CAS No.:100162-43-4
Molecular Formula:C₃₆H₆₆PbSn
Molecular Weight:824.83
Hs Code.:

Synonyms:tricyclohexylplumbyl-tricyclohexylstannane

Suppliers and Price of tricyclohexylplumbyl-tricyclohexylstannane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tricyclohexylplumbyl-tricyclohexylstannane

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Technology Process of tricyclohexylplumbyl-tricyclohexylstannane

There total 3 articles about tricyclohexylplumbyl-tricyclohexylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: tricyclohexylplumbyllithium

: 3091-32-5
tricyclohexyltin(IV) chloride

: 100162-43-4
tricyclohexylplumbyl-tricyclohexylstannane

Guidance literature:: In tetrahydrofuran; Pb-compound was dropwise added to soln. of Sn-compound in THF within 45 min at -50°C and stirred for 3 days to 0°C; mixture was stored under exclusion of air at -35°C overnight; soln. was cold filtered, ppt. dried in vac. and recrystd. from boiling benzene; elem. anal.;

Reference yield:

: 931-50-0
cyclohexylmagnesium bromide

: 100162-43-4
tricyclohexylplumbyl-tricyclohexylstannane

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: tetrahydrofuran

3: tetrahydrofuran

In tetrahydrofuran; diethyl ether;