Technology Process of 4-(methylthio)benzhydrylamine
There total 4 articles about 4-(methylthio)benzhydrylamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; zinc;
In
acetic acid;
for 3h;
Ambient temperature;
DOI:10.1135/cccc19920508
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 87 percent / NH2OH*HCl, NaOH / ethanol / 17 h / Heating
2: 47 percent / Zn, AcOH / acetic acid / 3 h / Ambient temperature
With
sodium hydroxide; hydroxylamine hydrochloride; acetic acid; zinc;
In
ethanol; acetic acid;
DOI:10.1135/cccc19920508
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 77 percent / AlCl3 / 1,2-dichloro-ethane
2: 87 percent / NH2OH*HCl, NaOH / ethanol / 17 h / Heating
3: 47 percent / Zn, AcOH / acetic acid / 3 h / Ambient temperature
With
sodium hydroxide; aluminium trichloride; hydroxylamine hydrochloride; acetic acid; zinc;
In
ethanol; acetic acid; 1,2-dichloro-ethane;
DOI:10.1135/cccc19920508
