C₂₄H₁₇NO₈

Base Information

• Chemical Name: C₂₄H₁₇NO₈
• CAS No.: 1256668-26-4
• Molecular Formula: C₂₄H₁₇NO₈
• Molecular Weight: 447.401
• Mol file: 1256668-26-4.mol

Synonyms:C₂₄H₁₇NO₈

Chemical Property of C₂₄H₁₇NO₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₁₇NO₈

There total 1 articles about C₂₄H₁₇NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

methyl 2-nitro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate (1256668-22-0) + C14H9IO3 (1256668-24-2) + acetic anhydride (108-24-7) → C24H17NO8 (1256668-26-4)

Guidance literature:

C₁₄H₉IO₃; acetic anhydride; With pyridine; dmap; In dichloromethane; for 2h; Inert atmosphere;

methyl 2-nitro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate; With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate tribasic; palladium diacetate; In tetrahydrofuran; water; at 80 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo101826p

Reference yield: 60.0%

C24H17NO8 (1256668-26-4) → C24H16BrNO8 (1256668-27-5)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 100 ℃; Inert atmosphere;

DOI:10.1021/jo101826p

upstream raw materials:

methyl 2-nitro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

C₁₄H₉IO₃

acetic anhydride

Downstream raw materials:

C₂₄H₁₆BrNO₈

Refernces