C₃₉H₇₂O₉Si₄

Base Information

Chemical Name:C₃₉H₇₂O₉Si₄
CAS No.:1394245-94-3
Molecular Formula:C₃₉H₇₂O₉Si₄
Molecular Weight:797.337
Hs Code.:

C<sub>39</sub>H<sub>72</sub>O<sub>9</sub>Si<sub>4</sub>

Synonyms:C₃₉H₇₂O₉Si₄

Suppliers and Price of C₃₉H₇₂O₉Si₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₇₂O₉Si₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₇₂O₉Si₄

There total 13 articles about C₃₉H₇₂O₉Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1394245-93-2
C₁₈H₃₈O₆Si₂

: 203118-32-5
(E)-3-(3,4-bis((tert-butyldimethylsilyl)oxy)phenyl)acrylic acid

: 1394245-94-3
C₃₉H₇₂O₉Si₄

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 4h; regioselective reaction;
DOI:10.1016/j.tet.2012.06.105

Reference yield:

: 142719-12-8
C₂₂H₃₆O₆Si

: 1394245-94-3
C₃₉H₇₂O₉Si₄

Guidance literature:: Multi-step reaction with 9 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 23 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.5 h / 20 °C

3: sodium hydride / tetrahydrofuran; mineral oil / 13 h / 0 - 20 °C

4: hydrogenchloride / water / 19 h / 20 - 50 °C

5: hydrogenchloride; water / 1,4-dioxane / 5.5 h / 80 °C

6: silver carbonate / toluene / 6 h / 80 °C

7: 1H-imidazole / N,N-dimethyl-formamide / 17 h / 20 °C

8: 20 % Pd(OH)2/C; hydrogen / ethanol / 1 h / 20 °C

9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 0 °C

With 1H-imidazole; hydrogenchloride; dmap; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; water; hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; silver carbonate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 6: Fetizon oxidation;
DOI:10.1016/j.tet.2012.06.105

Reference yield:

: 1394245-97-6
C₂₅H₃₂O₇

: 1394245-94-3
C₃₉H₇₂O₉Si₄

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / water / 19 h / 20 - 50 °C

2: hydrogenchloride; water / 1,4-dioxane / 5.5 h / 80 °C

3: silver carbonate / toluene / 6 h / 80 °C

4: 1H-imidazole / N,N-dimethyl-formamide / 17 h / 20 °C

5: 20 % Pd(OH)2/C; hydrogen / ethanol / 1 h / 20 °C

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 0 °C

With 1H-imidazole; hydrogenchloride; dmap; 20 % Pd(OH)2/C; water; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; silver carbonate; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 3: Fetizon oxidation;
DOI:10.1016/j.tet.2012.06.105