(5S)-5,6-dihydro-5-(1-methylethyl)-2-(2,3,4,5,6-pentafluorophenyl)-8H-1,2,4-Triazolo[3,4-c][1,4]oxazinium tetrafluoroborate

Base Information

• Chemical Name: (5S)-5,6-dihydro-5-(1-methylethyl)-2-(2,3,4,5,6-pentafluorophenyl)-8H-1,2,4-Triazolo[3,4-c][1,4]oxazinium tetrafluoroborate
• CAS No.: 1431323-18-0
• Molecular Formula: BF₄*C₁₄H₁₃F₅N₃O
• Molecular Weight: 421.073
• Mol file: 1431323-18-0.mol

Synonyms:(+)-(S)-5-isopropyl-2-(2,3,4,5,6-pentafluorophenyl)-6,8-dihydro-5H-[1,2,4]triazolo[3,4-c][1,4]oxazin-2-ium tetrafluoroborate

Chemical Property of (5S)-5,6-dihydro-5-(1-methylethyl)-2-(2,3,4,5,6-pentafluorophenyl)-8H-1,2,4-Triazolo[3,4-c][1,4]oxazinium tetrafluoroborate

Chemical Property:

• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

(5S)-5,6-Dihydro-5-(1-methylethyl)-2-(2,3,4,5,6-pentafluorophenyl)-8H-1,2,4-triazolo[3,4-c][1,4]oxaziniumtetrafluoroborate 97.88% ^*data from reagent suppliers

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Technology Process of (5S)-5,6-dihydro-5-(1-methylethyl)-2-(2,3,4,5,6-pentafluorophenyl)-8H-1,2,4-Triazolo[3,4-c][1,4]oxazinium tetrafluoroborate

There total 1 articles about (5S)-5,6-dihydro-5-(1-methylethyl)-2-(2,3,4,5,6-pentafluorophenyl)-8H-1,2,4-Triazolo[3,4-c][1,4]oxazinium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

(S)-5-isopropylmorpholin-3-one (127958-60-5) + orthoformic acid triethyl ester (122-51-0) + pentafluorophenyl hydrazine (828-73-9) → (+)-(S)-5-isopropyl-2-(2,3,4,5,6-pentafluorophenyl)-6,8-dihydro-5H-[1,2,4]triazolo[3,4-c][1,4]oxazin-2-ium tetrafluoroborate (1431323-18-0)

Guidance literature:

(S)-5-isopropylmorpholin-3-one; With trimethoxonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;

pentafluorophenyl hydrazine; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;

orthoformic acid triethyl ester; In chlorobenzene; at 130 ℃; for 48h; Reflux;

DOI:10.1021/ol400769t

upstream raw materials:

(S)-5-isopropylmorpholin-3-one

orthoformic acid triethyl ester

pentafluorophenyl hydrazine

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