4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine

Base Information

• Chemical Name: 4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine
• CAS No.: 810683-45-5
• Molecular Formula: C₁₆H₂₃N₃S
• Molecular Weight: 289.445

Synonyms:4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine

Chemical Property of 4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine

Chemical Property:

Purity/Quality:

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Technology Process of 4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine

There total 1 articles about 4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

guanidine hydrochloride (50-01-1) + 1,1-dimethylmercapto-5-(2,6,6-trimethyl-1-cyclohexene-1-yl)-penta-1,4-(Z)-dien-3-one → 4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine (810683-45-5)

Guidance literature:

In isopropyl alcohol; at 120 - 130 ℃; for 24h;

DOI:10.1016/j.ejmech.2004.03.007

Reference yield: 66.0%

4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine (810683-45-5) → (CH3)3C6H6CHCHC4H6N5

Guidance literature:

With hydrazine hydrate; for 24h; Heating;

DOI:10.1016/j.ejmech.2006.10.002

Reference yield: 50.0%

4-Methylsulfanyl-6-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-pyrimidin-2-ylamine (810683-45-5) → (CH3)3C6H6CHCHC4H3N3SO2CH3 (952419-04-4) + (CH3)3C6H6OCHCHC4H3N3SO2CH3

Guidance literature:

With Oxone; In tetrahydrofuran; water; at 20 ℃; for 4h;

DOI:10.1016/j.ejmech.2006.10.002

upstream raw materials:

guanidine hydrochloride

Downstream raw materials:

(CH₃)3C₆H₆CHCHC₄H₃N₃SO₂CH₃

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