5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

Base Information

Chemical Name:5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide
CAS No.:945240-99-3
Molecular Formula:C₂₈H₂₅N₃O₄
Molecular Weight:467.524
Hs Code.:

Synonyms:5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

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Chemical Property of 5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

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Technology Process of 5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

There total 3 articles about 5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 945244-18-8
1-(benzo[d][1,3]dioxol-5-yl)-N-(3-bromo-4-(cyanomethyl)phenyl)cyclopropane carboxamide

: 405520-68-5
4-(N,N-dimethylaminocarbonyl)phenylboronic acid

: 945240-99-3
5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

Guidance literature:: With potassium carbonate; Pd-FibreCat 1007; In N,N-dimethyl-formamide; at 150 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 945244-17-7
1-(benzo[d][1,3]dioxol-5-yl)-N-(3-bromo-4-(hydroxymethyl)phenyl)cyclopropanecarboxamide

: 945240-99-3
5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium cyanide; N-ethyl-N,N-diisopropylamine / acetonitrile

2: K₂CO₃ / N,N-dimethyl-formamide

With potassium cyanide; K₂CO₃; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 945244-47-3
methyl 4-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2-bromobenzoate

: 945240-99-3
5'-(1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamido)-2'-(cyanomethyl)-N,N-dimethylbiphenyl-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: potassium cyanide; N-ethyl-N,N-diisopropylamine / acetonitrile

3: K₂CO₃ / N,N-dimethyl-formamide

With potassium cyanide; K₂CO₃; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;