C₁₉H₃₂O₂Si

Base Information

• Chemical Name: C₁₉H₃₂O₂Si
• CAS No.: 1266621-77-5
• Molecular Formula: C₁₉H₃₂O₂Si
• Molecular Weight: 320.547
• Mol file: 1266621-77-5.mol

Synonyms:C₁₉H₃₂O₂Si

Chemical Property of C₁₉H₃₂O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₉H₃₂O₂Si

There total 1 articles about C₁₉H₃₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

triethylsilyl chloride (994-30-9) + (2R,3S)-1-Benzyloxy-3-methyl-pent-4-en-2-ol (635727-09-2) → C19H32O2Si (1266621-77-5)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

DOI:10.1002/chem.201002501

Reference yield: 86.0%

C19H32O2Si (1266621-77-5) + C22H46O3Si2 (1266621-76-4) → C39H74O5Si3

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 12h; Inert atmosphere; Reflux;

DOI:10.1002/chem.201002501

Reference yield:

C19H32O2Si (1266621-77-5) → C27H46O4Si (1266621-80-0)

Guidance literature:

Multi-step reaction with 4 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / Inert atmosphere; Reflux

2: hydrogen / ethyl acetate / 18 h / 760.05 Torr

3: pyridinium p-toluenesulfonate / methanol; dichloromethane / 3 h / 0 °C

4: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 0 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogen; pyridinium p-toluenesulfonate; In methanol; dichloromethane; ethyl acetate;

DOI:10.1002/chem.201002501

upstream raw materials:

triethylsilyl chloride

(2R,3S)-1-Benzyloxy-3-methyl-pent-4-en-2-ol

Downstream raw materials:

C₂₇H₄₆O₄Si

C₂₇H₄₆O₄Si

C₂₁H₃₂O₄

C₃₉H₇₆O₅Si₃