1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

Base Information

Chemical Name:1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone
CAS No.:191219-02-0
Molecular Formula:C₂₄H₂₀N₄O₂
Molecular Weight:396.448
Hs Code.:

Synonyms:1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

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Chemical Property of 1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

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Technology Process of 1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

There total 1 articles about 1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 613-94-5
benzoic acid hydrazide

: 33064-14-1
4-benzoyl-3-methyl-1-phenylpyrazol-5-one

: 191219-02-0
1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

Guidance literature:: In methanol; Reflux;
DOI:10.1002/ejic.201001083

Reference yield: 81.0%

: zinc(II) nitrate hexahydrate

: 191219-02-0
1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

: 1282522-09-1
[Zn(1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketonebenzoyl hydrazone-H)2]

Guidance literature:: With LiOH; In methanol; LiOH (0.1 mmol) added to soln. of org. ligand (0.1 mmol); Zn(NO3)2*6H2O (0.05 mmol) added; stirred (3 h); ppt. dissolved in DMF; MeOH added;; evapd. (room temp.);
DOI:10.1002/ejic.201001083

Reference yield: 79.0%

: gadolinium(III) chloride hydrate

: 191219-02-0
1-phenyl-3-methyl-5-hydroxy-4-pyrazolyl phenyl ketone benzoyl hydrazone

: 7732-18-5
water

: Gd⁽³⁺⁾*3C₆H₅C(O)NHNC(C₆H₅)C₃N₂(CH₃)(O)C₆H₅^(1-)*3H₂O=Gd(C₆H₅C(O)NHNC(C₆H₅)C₃N₂(CH₃)(O)(C₆H₅))3*3H₂O

Guidance literature:: With NaOH; In water; soln. of ligand heated at 50 °C with stirring, pH adjusted to 7 by aq. NaOH, soln. of lanthanide chloride added dropwise, stirred at 50 °C for 0.5 h; ppt. sepd. by suction filtration, washed (H2O), dried (vac.); elem. anal.;
DOI:10.1081/SIM-120005610